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Towards understanding the fatigue behaviour of Alloy 718 manufactured by Powder Bed Fusion processes
University West, Department of Engineering Science, Division of Subtractive and Additive Manufacturing. (PTW)ORCID iD: 0000-0002-8664-4573
2020 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Additive Manufacturing (AM) is a disruptive modern manufacturing process in which parts are manufactured in a layer-wise fashion. Among the metal AM processes, Powder Bed Fusion (PBF) technology — comprised of Electron Beam Powder Bed Fusion (EB-PBF) and Laser Beam Powder Bed Fusion (LB-PBF) —has opened up a design space that was formerly unavailable with conventionalmanufacturing processes. PBF processes offer several advantages; however, thesuitability of these processes to replace the conventional processes must be investigatedin detail. Therefore, understanding the AM process – post-processing –microstructure – property relationships is crucial for the manufacturing of high performance components. In this regard, only limited work has been done towards understanding the fatigue behaviour of PBF Alloy 718. The aim of this work, therefore, is to understand how the fatigue behaviour of PBF Alloy 718 is affected by its microstructure. Besides, the influence of the rough as-built surface is also investigated. In general, the <100> fibre texture along the build direction that resulted from PBF processing of Alloy 718 led to anisotropy in Young's modulus. Consequently,the fatigue performance under controlled amplitudes of strain was anisotropic such that the low-modulus direction had longer fatigue life and vice versa. This texture-induced elasticity-dependent anisotropic strain-life behaviour couldbe normalized by the pseudo-elastic stress vs fatigue life approach.Inclusions and defects had a detrimental effect on fatigue performance. Numerousfactors, such as their geometry, volume fraction, and distribution, determinedthe effect on fatigue behaviour. Hot Isostatic Pressing (HIP) eliminated most defect sand led to an improvement in fatigue performance. However, HIP did not alter the inclusions, which acted as crack initiation sites and reduced fatigue life. The rough as-built surface, which had numerous notch-like crack initiation sites, deteriorated fatigue performance; however, it lowered the scatter in fatigue life. Machining off the as-built surface improved fatigue life but increased the scatter.

Place, publisher, year, edition, pages
Trollhättan: University West , 2020. , p. 79
Series
PhD Thesis: University West ; 42
Keywords [en]
Fatigue; Additive Manufacturing; Powder Bed Fusion; Superalloy; Microstructure; Surface Roughness
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
URN: urn:nbn:se:hv:diva-16034ISBN: 978-91-88847-79-9 (print)ISBN: 978-91-88847-78-2 (print)OAI: oai:DiVA.org:hv-16034DiVA, id: diva2:1501299
Public defence
2020-12-08, Albertssalen, Trollhättan, 13:00 (English)
Opponent
Supervisors
Note

Tillstånd till elektronisk publicering finns för samtliga artiklar

Available from: 2020-11-16 Created: 2020-11-16 Last updated: 2020-11-16Bibliographically approved
List of papers
1. Anisotropic fatigue properties of Alloy 718 manufactured by Electron Beam Powder Bed Fusion
Open this publication in new window or tab >>Anisotropic fatigue properties of Alloy 718 manufactured by Electron Beam Powder Bed Fusion
2020 (English)In: International Journal of Fatigue, ISSN 0142-1123, E-ISSN 1879-3452, Vol. 141, article id 105898Article in journal (Refereed) Published
Abstract [en]

In this study, Alloy 718 specimens manufactured by Electron Beam Powder Bed Fusion process are subjected to two different post-treatments to have different microstructural features. Low cycle fatigue testing has been performed both parallel and transverse to the build direction. EB-PBF Alloy 718 exhibits anisotropic fatigue behaviour; the fatigue life is better along the parallel direction compared to the transverse direction. The anisotropy in fatigue life is related to the anisotropy in the Young’s modulus. The pseudo-elastic stress vs. fatigue life approach is presented as a potential solution to handle anisotropy in fatigue life assessment of additively manufactured engineering components. © 2020 The Authors

Place, publisher, year, edition, pages
Elsevier, 2020
Keywords
Anisotropy; Elastic moduli; Electron beams; Fatigue testing, Build direction; Engineering components; Fatigue behaviour; Fatigue life assessment; Fatigue properties; Low cycle fatigue testing; Microstructural features; Post treatment, Fatigue of materials
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-15776 (URN)10.1016/j.ijfatigue.2020.105898 (DOI)000571197300001 ()2-s2.0-85089796084 (Scopus ID)
Funder
Knowledge Foundation, 20160281
Available from: 2020-09-08 Created: 2020-09-08 Last updated: 2020-11-16Bibliographically approved
2. Influence of defects and as-built surface roughness on fatigue properties of additively manufactured Alloy 718
Open this publication in new window or tab >>Influence of defects and as-built surface roughness on fatigue properties of additively manufactured Alloy 718
2018 (English)In: Materials Science & Engineering: A, ISSN 0921-5093, E-ISSN 1873-4936, Vol. 735, p. 463-474Article in journal (Refereed) Published
Abstract [en]

Electron beam melting (EBM) and Selective Laser Melting (SLM) are powder bed based additive manufacturing (AM) processes. These, relatively new, processes offer advantages such as near net shaping, manufacturing complex geometries with a design space that was previously not accessible with conventional manufacturing processes, part consolidation to reduce number of assemblies, shorter time to market etc. The aerospace and gas turbine industries have shown interest in the EBM and the SLM processes to enable topology-optimized designs, parts with lattice structures and part consolidation. However, to realize such advantages, factors affecting the mechanical properties must be well understood – especially the fatigue properties. In the context of fatigue performance, apart from the effect of different phases in the material, the effect of defects in terms of both the amount and distribution and the effect of “rough” as-built surface must be studied in detail. Fatigue properties of Alloy 718, a Ni-Fe based superalloy widely used in the aerospace engines is investigated in this study. Four point bending fatigue tests have been performed at 20 Hz in room temperature at different stress ranges to compare the performance of the EBM and the SLM material to the wrought material. The experiment aims to assess the differences in fatigue properties between the two powder bed AM processes as well as assess the effect of two post-treatment methods namely – machining and hot isostatic pressing (HIP). Fractography and metallography have been performed to explain the observed properties. Both HIPing and machining improve the fatigue performance; however, a large scatter is observed for machined specimens. Fatigue properties of SLM material approach that of wrought material while in EBM material defects severely affect the fatigue life. © 2018 Elsevier B.V.

Keywords
Additive manufacturing, Alloy 718, Fatigue, Surface roughness, Hot isostatic pressing, 3D printers, Bending tests, Binary alloys, Fatigue testing, Fighter aircraft, Fracture mechanics, Gas turbines, Hot isostatic pressing, Iron alloys, Mechanical properties, Melting, Nickel alloys, Sintering, Surface roughness, Alloy 718, Conventional manufacturing, Fatigue performance, Gas turbine industry, Lattice structures, Manufacturing complex, Post-treatment method, Selective laser melting, Fatigue of materials
National Category
Manufacturing, Surface and Joining Technology
Research subject
ENGINEERING, Manufacturing and materials engineering; Production Technology
Identifiers
urn:nbn:se:hv:diva-12956 (URN)10.1016/j.msea.2018.08.072 (DOI)000447117300055 ()2-s2.0-85052655828 (Scopus ID)
Funder
Knowledge Foundation, 20160281
Note

Available online 23 August 2018

Available from: 2018-09-27 Created: 2018-09-27 Last updated: 2020-11-16Bibliographically approved
3. Microstructural influence on fatigue crack propagation during high cycle fatigue testing of additively manufactured Alloy 718
Open this publication in new window or tab >>Microstructural influence on fatigue crack propagation during high cycle fatigue testing of additively manufactured Alloy 718
Show others...
2019 (English)In: Materials Characterization, ISSN 1044-5803, E-ISSN 1873-4189, Vol. 149, p. 82-94Article in journal (Refereed) Published
Abstract [en]

A study of the microstructure of additively manufactured Alloy 718 was performed in order to better understand the parameters that have an influence on the fatigue properties of the material. The specimens were manufactured using two powder bed fusion techniques – Electron Beam Melting (EBM) and Selective Laser Melting (SLM). Four point bending fatigue tests were performed at room temperature with a stress ratio of R = 0.1 and 20 Hz frequency, on material that was either in hot isostatically pressed (HIP) and solution treated and aged (STA) condition or in STA condition without a prior HIP treatment. The grains in the SLM material in the HIP + STA condition have grown considerably both in the hatch and the contour regions; EBM material, in contrast, shows grain growth only in the contour region. Fractographic analysis of the specimens in HIP + STA condition showed a faceted appearance while the specimens in STA condition showed a more planar crack appearance. The crack propagation occurred in a transgranular mode and it was found that precipitatessuch as NbC, TiN or δ-phase, when present, did not affect the crack path. The areas with larger grains corresponded to the faceted appearance of the fracture surface. This could be attributed to the plastic zone ahead of the crack tip being confined within one grain, in case of the larger grains, which promotes single shear crack growth mode

Keywords
Electron beam melting, Selective laser melting, Alloy 718, Fatigue crack propagation, Microstructure, Hot isostatic pressing
National Category
Manufacturing, Surface and Joining Technology
Research subject
ENGINEERING, Manufacturing and materials engineering
Identifiers
urn:nbn:se:hv:diva-13460 (URN)10.1016/j.matchar.2019.01.018 (DOI)000475837800008 ()2-s2.0-85060346504 (Scopus ID)
Funder
Knowledge Foundation, 20160281
Available from: 2019-02-04 Created: 2019-02-04 Last updated: 2020-11-16Bibliographically approved
4. Additive Manufacturing of Alloy 718 via Electron Beam Melting: Effect of Post-Treatment on the Microstructure and the Mechanical Properties.
Open this publication in new window or tab >>Additive Manufacturing of Alloy 718 via Electron Beam Melting: Effect of Post-Treatment on the Microstructure and the Mechanical Properties.
2018 (English)In: Materials, E-ISSN 1996-1944, Vol. 12, no 1, article id E68Article in journal (Refereed) Published
Abstract [en]

Alloy 718 finds application in gas turbine engine components, such as turbine disks, compressor blades and so forth, due to its excellent mechanical and corrosion properties at elevated temperatures. Electron beam melting (EBM) is a recent addition to the list of additive manufacturing processes and has shown the capability to produce components with unique microstructural features. In this work, Alloy 718 specimens were manufactured using the EBM process with a single batch of virgin plasma atomized powder. One set of as-built specimens was subjected to solution treatment and ageing (STA); another set of as-built specimens was subjected to hot isostatic pressing (HIP), followed by STA (and referred to as HIP+STA). Microstructural analysis of as-built specimens, STA specimens and HIP+STA specimens was carried out using optical microscopy and scanning electron microscopy. Typical columnar microstructure, which is a characteristic of the EBM manufactured alloy, was observed. Hardness evaluation of the as-built, STA and HIP+STA specimens showed that the post-treatments led to an increase in hardness in the range of ~50 HV1. Tensile properties of the three material conditions (as-built, STA and HIP+STA) were evaluated. Post-treatments lead to an increase in the yield strength (YS) and the ultimate tensile strength (UTS). HIP+STA led to improved elongation compared to STA due to the closure of defects but YS and UTS were comparable for the two post-treatment conditions. Fractographic analysis of the tensile tested specimens showed that the closure of shrinkage porosity and the partial healing of lack of fusion (LoF) defects were responsible for improved properties. Fatigue properties were evaluated in both STA and HIP+STA conditions. In addition, three surface conditions were also investigated, namely the 'raw' as-built surface, the machined surface with the contour region and the machined surface without the contour region. Machining off the contour region completely together with HIP+STA led to significant improvement in fatigue performance.

Keywords
Alloy 718, electron beam melting, fatigue properties, microstructure, tensile properties, texture
National Category
Manufacturing, Surface and Joining Technology
Research subject
ENGINEERING, Manufacturing and materials engineering; Production Technology
Identifiers
urn:nbn:se:hv:diva-13364 (URN)10.3390/ma12010068 (DOI)000456410200068 ()30585242 (PubMedID)2-s2.0-85059182911 (Scopus ID)
Funder
Knowledge Foundation, 20160281
Available from: 2019-01-08 Created: 2019-01-08 Last updated: 2024-07-04Bibliographically approved
5. Microstructure tailoring in Electron Beam Powder Bed Fusion Additive Manufacturing and its potential consequences
Open this publication in new window or tab >>Microstructure tailoring in Electron Beam Powder Bed Fusion Additive Manufacturing and its potential consequences
Show others...
2019 (English)In: Results in Materials, E-ISSN 2590-048X, Vol. 1Article in journal (Refereed) Published
Abstract [en]

Electron Beam Powder Bed Fusion process for Alloy 718 was investigated, in the sense of microstructural evolution with varying process conditions. The existence of a geometric relationship between the melt front and the processing parameters was observed. By understanding and capitalizing on this relationship, it was possible to obtain columnar, equiaxed or bimodal microstructure.

Place, publisher, year, edition, pages
Elsevier, 2019
Keywords
Alloy 718, Texture, Microstructure, Additive manufacturing, Powder bed fusion
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology; ENGINEERING, Manufacturing and materials engineering
Identifiers
urn:nbn:se:hv:diva-14331 (URN)10.1016/j.rinma.2019.100017 (DOI)
Available from: 2019-08-26 Created: 2019-08-26 Last updated: 2024-06-27Bibliographically approved

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Balachandramurthi, Arun Ramanathan

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