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Thalavai Pandian, K., Lindgren, E., Roychowdhury, S., Neikter, M., Hansson, T. & Pederson, R. (2024). Characterization of surface asperities to understand its effect on fatigue life of electron beam powder bed fusion manufactured Ti-6Al-4 V. International Journal of Fatigue, 188, Article ID 108516.
Open this publication in new window or tab >>Characterization of surface asperities to understand its effect on fatigue life of electron beam powder bed fusion manufactured Ti-6Al-4 V
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2024 (English)In: International Journal of Fatigue, ISSN 0142-1123, E-ISSN 1879-3452, Vol. 188, article id 108516Article in journal (Refereed) Published
Abstract [en]

Surface asperities play a leading role in determining the fatigue life of as-built Ti-6Al-4 V components manufactured by electron beam powder bed fusion (PBF-EB). Several roughness parameters are available to characterize the surface asperities This study focuses on identifying the surface roughness parameter that correlates best with fatigue life. To this end, several fatigue test specimens were manufactured using the PBF-EB process and utilizing different contour melting strategies, thus producing as-built surfaces with varying roughness. The focus variation microscopy technique was employed to obtain surface roughness parameters for the as-built surfaces. Selected specimens were characterized using x-ray computed tomography (XCT). Tomography can detect surface-connected features obscured by other parts of the surface that are not visible through optical microscopy. The fatigue life of all specimens was determined using four-point bend testing. Through regression model analysis, maximum pit height (Sv) was identified as the statistically significant roughness parameter with the best fit affecting fatigue life. The fracture zone was closely inspected based on the data collected through XCT prior to fatigue tests. This led to another estimate of the worst-case value for the statistically significant roughness parameter Sv. The Sv parameter values obtained from optical microscopy and XCT were used as the initial crack size in a crack growth model to predict fatigue life. It is observed that life estimates based solely on optical measurements of Sv can be overly optimistic, a situation that must be avoided in predictive design calculations.

Place, publisher, year, edition, pages
Elsevier, 2024
Keywords
Electron beam melting, Additive manufacturing, Surface roughness, Fatigue life, X-ray computed tomography
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-22393 (URN)10.1016/j.ijfatigue.2024.108516 (DOI)001280969100001 ()2-s2.0-85199366115 (Scopus ID)
Funder
Vinnova, 2023-01584
Note

CC-BY 4.0

VINNOVA has financially supported the current research through the “Swedish National Program for Aeronautical Technology” (project #:2019-02741 and 2023-01584). 

Available from: 2024-09-09 Created: 2024-09-09 Last updated: 2024-09-09
Squillaci, L., Neikter, M., Hansson, T., Harlin, P., Niklasson, F. & Pederson, R. (2024). Extending powder particle size distribution of laser powder bed fusion Ti-6Al-4V: investigation of single tracks and multilayer experiments.. In: Proceedings of the 15th World Conference on Titanium Chapter 1: Additive Manufacturing & Repair Technology. Paper presented at The 15th World Titanium Conference, Edinburgh, 12–16 June 2023 (pp. 124-129).
Open this publication in new window or tab >>Extending powder particle size distribution of laser powder bed fusion Ti-6Al-4V: investigation of single tracks and multilayer experiments.
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2024 (English)In: Proceedings of the 15th World Conference on Titanium Chapter 1: Additive Manufacturing & Repair Technology, 2024, p. 124-129Conference paper, Published paper (Other academic)
Abstract [en]

Laser powder bed fusion (PBF-LB) is one of the most widespread additive manufacturing (AM) methods, spanning multiple industrialsectors such as medical, automotive and more recently aerospace. Current limitations to its large-scale adoption include low build rates,machining often required and consolidation via hot isostatic pressing (HIP). Productivity enhancement of PBF-LB has been investigated extensively and among the strategies adopted, that of combining high-speed parameters with HIP to achieve full density, has proven to beviable. This study puts forward a new approach for Ti-6Al-4V material, investigating if employing a wide particle size distribution (PSD)of the powder, with a range between 15 to 90μm, with a high layer thickness achieves comparable levels of bulk density, whilst improvingthe sustainability of the overall process and decreasing build times. If packing density can be improved by ensuring a more varied spreadof particle sizes, the thermal conductivity of the powder bed increases. Combination of small and large diameter particles would result in a reduction of the number of interparticle cavities upon powder spreading, therefore enhancing the contact and the efficiency of melting between neighbouring particles, upon laser heating. An EOS M290 machine was used to establish a processing window for the extendedPSD and increased layer thickness. Laser power, scanning velocity and hatch distance were varied to identify and exclude parametervalues that render extremes such as lack of fusion or keyholing defects. Single, multiple tracks and cubes were produced as part of a studythat aims to characterise the material’s response in terms of microstructure, defect density and hardness. It was possible to establish correspondence between tracks and cubes behaviour and isolate a design region that yielded minimal porosity.

Keywords
Laser powder bed fusion (PBF-LB), Ti-6Al-4V, powder size distribution (PSD), productivity enhancement, microstructure
National Category
Manufacturing, Surface and Joining Technology Metallurgy and Metallic Materials
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-22574 (URN)10.7490/f1000research.1119881.1 (DOI)
Conference
The 15th World Titanium Conference, Edinburgh, 12–16 June 2023
Note

CC-BY 4.0

Available from: 2024-11-04 Created: 2024-11-04 Last updated: 2024-11-04
Tolvanen, S., Pederson, R. & Klement, U. (2024). Microstructure and Mechanical Properties of Ti-6Al-4V Welds Produced with Different Processes.. Materials, 17(4), Article ID 782.
Open this publication in new window or tab >>Microstructure and Mechanical Properties of Ti-6Al-4V Welds Produced with Different Processes.
2024 (English)In: Materials, ISSN 1996-1944, Vol. 17, no 4, article id 782Article in journal (Refereed) Published
Abstract [en]

The effect of defects and microstructure on the mechanical properties of Ti-6Al-4V welds produced by tungsten inert gas welding; plasma arc welding; electron beam welding; and laser beam welding was studied in the present work. The mechanical properties of different weld types were evaluated with respect to micro hardness; yield strength; ultimate tensile strength; ductility; and fatigue at room temperature and at elevated temperatures (200 °C and 250 °C). Metallographic investigation was carried out to characterize the microstructures of different weld types, and fractographic investigation was conducted to relate the effect of defects on fatigue performance. Electron and laser beam welding produced welds with finer microstructure, higher tensile ductility, and better fatigue performance than tungsten inert gas welding and plasma arc welding. Large pores, and pores located close to the specimen surface, were found to be most detrimental to fatigue life.

Place, publisher, year, edition, pages
MDPI, 2024
Keywords
defects, fatigue, microstructure, porosity, titanium alloys, welding
National Category
Manufacturing, Surface and Joining Technology Other Materials Engineering
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-21314 (URN)10.3390/ma17040782 (DOI)001172260100001 ()38399033 (PubMedID)2-s2.0-85185835158 (Scopus ID)
Note

CC-BY 4.0

The authors would like to acknowledge the financial support of NFFP (the SwedishNational Program for Aeronautical Technology)

Available from: 2024-05-20 Created: 2024-05-20 Last updated: 2024-11-21Bibliographically approved
Pederson, R., Andersson, J. & Joshi, S. V. (2023). Additive Manufacturing of High-Performance Metallic Materials (1.ed.). Elsevier
Open this publication in new window or tab >>Additive Manufacturing of High-Performance Metallic Materials
2023 (English)Book (Refereed)
Place, publisher, year, edition, pages
Elsevier, 2023. p. 744 Edition: 1.
Keywords
Feedstock, processing, monitoring modeling, simulation
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-20865 (URN)9780323918855 (ISBN)9780323913829 (ISBN)
Available from: 2023-11-22 Created: 2023-11-22 Last updated: 2024-01-03Bibliographically approved
Isoaho, J., Dordlofva, C., Segerstark, A., Harlin, P. & Pederson, R. (2023). Applications of additive manufacturing: Selected case studies and future prospects (1ed.). In: Pederson, Robert, Andersson, Joel & Joshi, Shrikant V. (Ed.), Additive Manufacturing of High-Performance metallic Materials: (pp. 676-716). Elsevier
Open this publication in new window or tab >>Applications of additive manufacturing: Selected case studies and future prospects
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2023 (English)In: Additive Manufacturing of High-Performance metallic Materials / [ed] Pederson, Robert, Andersson, Joel & Joshi, Shrikant V., Elsevier, 2023, 1, p. 676-716Chapter in book (Refereed)
Abstract [en]

From an industrial standpoint, cost is of one of the most important drivers for utilizing new technologies such as additive manufacturing (AM). Other important drivers for why AM can be an advantageous technology for component manufacturing is decreased manufacturing lead time, rapid demonstration capability, freedom of design/geometry, advancing technology development, and not least sustainability in terms of both material utilization and improved part/system performance. In this chapter, six selected “case studies” are compiled, in which AM techniques have been used to manufacture components for actual applications. In some case studies, a comparison between the additive manufacturing route and the corresponding conventional manufacturing route is also included.

Place, publisher, year, edition, pages
Elsevier, 2023 Edition: 1
Keywords
Cost, Component manufacturing, Demonstrator, Design freedom, Manufacturing lead time, Sustainability, Superalloys, Technology development, Titanium alloys
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-21093 (URN)9780323918855 (ISBN)9780323913829 (ISBN)
Available from: 2023-12-19 Created: 2023-12-19 Last updated: 2024-01-03Bibliographically approved
Squillaci, L., Neikter, M., Hansson, T., Harlin, P., Niklasson, F. & Pederson, R. (2023). Extending powder particle size distribution of laser powder bed fusion Ti-6Al-4V: investigation of single tracks and multilayer experiments. In: : . Paper presented at 15th World Titanium Conference, June 2023, Edinburgh, United Kingdom.
Open this publication in new window or tab >>Extending powder particle size distribution of laser powder bed fusion Ti-6Al-4V: investigation of single tracks and multilayer experiments
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2023 (English)Conference paper, Oral presentation with published abstract (Other academic)
Abstract [en]

This paper explores the effects of varying process parameters (i.e., laser power, laser scanning speed, hatch distance) on the characteristics of single tracks, triple tracks and cubes, in order to provide answers to Research Question 1. A full factorial DoE approach was adopted to produce the experiments. Data was extracted from different sources to find correlations between tracks and multilayer geometries. A digital microscope was used to obtain height profiles, whilst polished/etched cross sections cut parallel to the build direction were imaged using a LOM to obtain measurements of track height, width, melt pool depth, subsurface porosity and residual defect content in cubes. Track height was found to exceed the recoated value of 70μm for both single and triple tracks. The width of single tracks showed a clear upward trend when displayed against VED, showing a lateral expansion as energy input increased. It was also revealed that single tracks expand laterally as they grow above the substrate, indicating swelling. The melt pool depth showed a steady upward trend when plotted against LED, though less systematic than track width. A martensitic microstructure was detected, with hierarchical α’ needles growing at prescribed crystallographic directions within vertical prior-β grains. A large portion of spatter particles and unmelted powder granules were detected on the substrate and tracks, with many accumulating on the side of the tracks forming a denudation zone.

Keywords
extendign powder, laser powder
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-20988 (URN)
Conference
15th World Titanium Conference, June 2023, Edinburgh, United Kingdom
Note

This paper is under review och will be published in Proceedings.

Available from: 2023-11-24 Created: 2023-11-24 Last updated: 2024-01-08Bibliographically approved
Thalavai Pandian, K., Neikter, M., Bahbou, F., Ganvir, A., Hansson, T. & Pederson, R. (2023). Fatigue behavior of low-temperature hot isostatic pressed electron beam powder bed fusion manufactured Ti-6Al-4 V. Journal of Alloys and Compounds, 962, Article ID 171086.
Open this publication in new window or tab >>Fatigue behavior of low-temperature hot isostatic pressed electron beam powder bed fusion manufactured Ti-6Al-4 V
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2023 (English)In: Journal of Alloys and Compounds, ISSN 0925-8388, Vol. 962, article id 171086Article in journal (Refereed) Published
Abstract [en]

Ti-6Al-4 V finds application in the fan and compressor modules of gas turbine engines due to its high specific strength. Ti-6Al-4 V components manufactured using one of the additive manufacturing (AM) techniques, the electron beam powder bed fusion (PBF-EB) process, has been an active area of research in the past decade. The fatigue life of such PBF-EB built Ti-6Al-4 V components is improved by hot isostatic pressing (HIP) treatment typically performed at about 920 ˚C. The HIP treatment at 920 ˚C results in coarsening of α laths and reduced static strength and therefore a low-temperature HIP treatment is performed at about 800 ˚C to limit the impact on static mechanical properties. In the present work, the low cycle fatigue and fatigue crack growth behavior of such a modified HIP (low-temperature HIP) treated material is assessed and compared with the respective data for the standard HIP-treated material. The modified HIP-treated material has fatigue performance comparable to the standard HIP-treated material. This work suggests that the modified HIP treatment improves the static mechanical properties without significantly impacting the fatigue performance. Also, fatigue life predictions were made from the measured defect size at the crack initiation site using a linear elastic fracture mechanics tool. The life predictions show good agreement with the experimental values for defects greater than the intrinsic crack length, where life is well predicted by large-crack growth methodology. 

Place, publisher, year, edition, pages
Elsevier, 2023
Keywords
Additive manufacturing Electron beam melting Hot isostatic pressing Low cycle fatigue Fatigue crack growth Ti-6Al-4 V
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-20691 (URN)10.1016/j.jallcom.2023.171086 (DOI)001031870200001 ()2-s2.0-85163861805 (Scopus ID)
Funder
Vinnova, 2019-02741
Note

CC BY 4.0

Available from: 2023-09-06 Created: 2023-09-06 Last updated: 2024-04-23Bibliographically approved
Pederson, R., Andersson, J., Joshi, S. V., Neikter, M. & Isoaho, J. (2023). Metal additive manufacturing: Motivation, process portfolio, and application potential (1ed.). In: Pederson, Robert, Andersson, Joel & Joshi, Shrikant V. (Ed.), Additive Manufacturing of High-Performance metallic Materials: (pp. 20-40). Elsevier
Open this publication in new window or tab >>Metal additive manufacturing: Motivation, process portfolio, and application potential
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2023 (English)In: Additive Manufacturing of High-Performance metallic Materials / [ed] Pederson, Robert, Andersson, Joel & Joshi, Shrikant V., Elsevier, 2023, 1, p. 20-40Chapter in book (Refereed)
Abstract [en]

The idea of adding material only where needed to manufacturesolid metallic high-performing components is intriguing andone of the main reasons for the great interest in additivemanufacturing (AM) around the world. Especially whensustainability comes into play, as in recent times more thanever, AM technology is most appropriate since it enables almostfull material utilization with minimal waste. From an economicstandpoint, this becomes particularly advantageous for moreexpensive materials such as superalloys and titanium alloys.However, the route of going from a CAD drawing of a part to anadditively manufactured final component that is qualified and inserial production involves numerous challenges. The intentionof this book is to shed light on and explain some of theassociated challenges beginning with the importance of thestarting material and how it is manufactured, i.e., wire orpowder, continuing into description of the conventional andPederson, R., Andersson, J., & Joshi, S. (2023). Additive manufacturing of high-performance metallic materials. Elsevier.Created from vast-ebooks on 2024-01-08 16:09:20. Copyright © 2023. Elsevier. All rights reserved.most commonly used AM processes, followed by postbuildtreatments and nondestructive evaluations, to eventuallyproduce the final part with mechanical performance consistentwith the application requirements. In the end, selected realindustry examples of AM parts for actual applications will bepresented

Place, publisher, year, edition, pages
Elsevier, 2023 Edition: 1
Keywords
Additive manufacturing; Superalloys; Titanium alloys; Powder; Wire; Postbuild treatment; Nondestructive evaluation; Mechanical properties
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-21065 (URN)9780323918855 (ISBN)9780323913829 (ISBN)
Available from: 2023-12-14 Created: 2023-12-14 Last updated: 2024-01-26Bibliographically approved
Mahade, S., Bhattacharya, P., Tolvanen, S., Pederson, R. & Neikter, M. (2023). Processing of high-performance materials by laser directed energy deposition with wire (1.ed.). In: Pederson, Robert, Andersson, Joel & Joshi, Shrikant V. (Ed.), Additive Manufacturing of High-Performance metallic Materials: (pp. 260-305). Elsevier
Open this publication in new window or tab >>Processing of high-performance materials by laser directed energy deposition with wire
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2023 (English)In: Additive Manufacturing of High-Performance metallic Materials / [ed] Pederson, Robert, Andersson, Joel & Joshi, Shrikant V., Elsevier, 2023, 1., p. 260-305Chapter in book (Refereed)
Abstract [en]

Processing of metallic materials by Laser Directed Energy Deposition (LDED), with Wire (w) as the feedstock, enables the manufacturing of high precision, near-net shape components that require minimal postmachining, without compromising the performance. L-DEDw has also shown the capability to add intricate features on large structures, which makes it an attractive fabrication technique for aerospace application. The key merits of wire as the feedstock when compared to powder include; higher deposition rates, low porosity in the deposited material, excellent surface finish, and, ∼ 100% utilization of the feedstock. However, despite the attractive merits, the difference in solidification rates during L-DEDw processing when compared to other fabrication routes could induce high residual stresses, which can be detrimental to the integrity of cracksensitive alloys. Additionally, there exists an inherent challenge during L-DEDw fabrication, where controlling the process variables to ensure stable deposition conditions becomes essential to achieve repeatable, and desired results. The recent advancements in the area of monitoring and control systems, and their integration with L-DEDw processing, have enabled to overcome the processing instability related challenges. Furthermore, different L-DEDw processing strategies for alleviating residual stresses (tensile) accumulation in the deposits are discussed, which could enable defectfree, high-performance component fabrication. Although the utilization of L-DEDw for processing diverse alloy systems has been explored in the literature, the current chapter's scope is restricted to L-DEDw processing of Nickel-based and Titanium-based alloys, which are often utilized in the aeroengine. This work aims to provide a holistic perspective and shed light on the state-of-the-art, recent developments, sustainability aspects and future directions for L-DEDw processed, highperformance Ni-based and Ti-based alloys.

Place, publisher, year, edition, pages
Elsevier, 2023 Edition: 1.
Keywords
Laser directed energy deposition with wire; Process parameters; Microstructure; Residual stress; Nibased superalloys; Ti-based alloys; Hot cracking; Lack of fusion
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-21072 (URN)9780323918855 (ISBN)9780323913829 (ISBN)
Available from: 2023-12-14 Created: 2023-12-14 Last updated: 2024-01-12Bibliographically approved
Adegoke, O., Kumara, C., Thuvander, M., Deirmina, F., Andersson, J., Brodin, H., . . . Pederson, R. (2023). Scanning electron microscopy and atom probe tomography characterization of laser powder bed fusion precipitation strengthening nickel-based superalloy. Micron, 171, Article ID 103472.
Open this publication in new window or tab >>Scanning electron microscopy and atom probe tomography characterization of laser powder bed fusion precipitation strengthening nickel-based superalloy
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2023 (English)In: Micron, ISSN 0968-4328, E-ISSN 1878-4291, Vol. 171, article id 103472Article in journal (Refereed) Epub ahead of print
Abstract [en]

Atom probe tomography (APT) was utilized to supplement scanning electron microscopy (SEM) characterizationof a precipitation strengthening nickel-based superalloy, Alloy 247LC, processed by laser powder bed fusion (LPBF). It was observed that the material in the as-built condition had a relatively high strength. Using both SEMand APT, it was concluded that the high strength was not attributed to the typical precipitation strengtheningeffect of γ’. In the absence of γ’ it could be reasonably inferred that the numerous black dots observed in thecells/grains with SEM were dislocations and as such should be contributing significantly to the strengthening.Thus, the current investigation demonstrated that relatively high strengthening can be attained in L-PBF even inthe absence of precipitated γ’. Even though γ’ was not precipitated, the APT analysis displayed a nanometer scalepartitioning of Cr that could be contributing to the strengthening. After heat-treatment, γ’ was precipitated and itdemonstrated the expected high strengthening behavior. Al, Ta and Ti partitioned to γ’. The strong partitioningof Ta in γ’ is indicative that the element, together with Al and Ti, was contributing to the strain-age crackingoccurring during heat-treatment. Cr, Mo and Co partitioned to the matrix γ phase. Hf, Ta, Ti and W were found inthe carbides corroborating previous reports that they are MC. 

Keywords
CM247LC, Superalloy, Additive manufacturing, atom probe tomography, Scanning electron microscopy, gamma prime
National Category
Manufacturing, Surface and Joining Technology
Research subject
Production Technology
Identifiers
urn:nbn:se:hv:diva-20014 (URN)10.1016/j.micron.2023.103472 (DOI)000999885100001 ()37146362 (PubMedID)2-s2.0-85154065448 (Scopus ID)
Available from: 2023-06-01 Created: 2023-06-01 Last updated: 2024-01-15Bibliographically approved
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ORCID iD: ORCID iD iconorcid.org/0000-0002-7675-7152

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